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Kumpulan Laporan Praktikum Analisa Kulit

Kumpulan Laporan Praktikum Analisa Kulit

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Published by: Hidayatullah on Mar 10, 2010
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06/13/2013

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1.Analisa Kesadahan Air
Air + Indikator MO = berwarna orange
Larutan dititrasi = berwarna merah sindur
Diket:

V titran sampel (b) = 9,5 ml
V titran blangko (c) = 24,6 ml
Titrasi I (a) = 3,9 ml
N HCl = 0,1 N
Maka:
Kesadahan sementara = a ml x N HCl x 28 o

D
= 3,9 ml x 0,1 N x 28
= 10,92

Kesadahan jumlah

= (c ml – 2 b ml) x N HCl x 28o

D

= (24,6 ml - 9,5 ml) x 0,1 N x 28
= 42,28
Kesadahan tetap= Kesadahan jumlah - Kesadahan sementara
= 42,28 - 10,92
= 31,36

2.Analisa Besi secara Kualitatif
Sampel + HNO3 = berwarna bening
Larutan + Lar kalium rodanida = berwarna bening
Hasil analisa larutan tetap bening.
3.Analisa pH

pH air sampel yang dicek dengan kertas pH adalah 7
pH air sampel yang dicek dengan pH meter adalah 7,7

[ANALISA BAHAN KULIT. TBKKP.07/IV]July , 2009

4.Analisa Kadar Clorida
Hasil analisa kualitatif = larutan menghasilkan endapan dan berwarna keruh.
Hasil analisa kuantitatif =
Perhitungan :
V Contoh air : 10 ml
V titran

: 0,5 ml
N KCNS : 0,1 N
V AgNO3 yang bereaksi : (10 – 0,5) ml = 9,5 ml
Maka:
Kadar Cl = 1000/10 x (10-b) ml x 0,1 N x 58,5
= 5557,5 ml
5.Kekeruhan
Sampel yang tidak disaring (a):
Berat cawan

= 41,091 gr
Berat cawan + sampel = 41,1214 gr
Endapan = (Berat cawan + sampel) - Berat cawan
= 41,1214 gr - 41,091 gr
= 0,0304 gr
Sampel yang disaring (b):
Berat cawan

= 36,2176 gr

Berat cawan + sampel = 36,2452 gr
Endapan= (Berat cawan + sampel) - Berat cawan
= 36,2452 gr - 36,2176 gr
= 0,0276 gr

Maka:
Kekeruhan = (Endapan a – Endapan b) x 1000/25 ml
= (0,0304 gr - 0,0276 gr) x 1000/25 ml
= 0,112 gram

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